Chemical Processing Equipment

Introduction

Chemical process equipment manufacturing is the oldest division of Dalal Engineering. The present range includes Wiped Film Evaporators (WFE) and Supertors.

Wiped Film Evaporator (WFE / TFE / ATFE)

Introduction

The Wiped Film Evaporator (WFE) - also referred to as a Thin Film Evaporator (TFE) or Agitated Thin Film Evaporator (ATFE) - is the versatile product of Dalal Engineering's (Chemical) Process Equipment Division. Designed for evaporation, concentration, distillation, stripping, dehydration, and deodorization, the Wiped Film Evaporator (WFE) is meant for feed streams that are heat-sensitive, viscous, or prone to fouling. The equipment accommodates a very wide range of feed compositions — from as low as 0.25% up to over 99% solute/non-volatile concentration - making it a versatile solution across different industry segments - agrochemical, adhesives, bulk drugs, fatty acids/oleochemicals, fragrances & perfumery, polymers, specialty chemical, use lube oil reclamation, etc.

As an experienced evaporator manufacturer in India, Dalal Engineering brings decades of application knowledge and customization to every WFE manufacturing. (Customization for every case of Thin Film Distillation Equipment manufacturing project.)

Working Principle

Operation of the wiped film evaporator (WFE) is both smooth and effective. Feed material is introduced at the top of the unit and spread uniformly over the heated inner shell surface by a rotating distribution plate. Specially engineered wipers continuously wipe the feed, create a thin film, and renew this thin film, ensuring efficient heat transfer even for viscous fluids — a defining characteristic of all thin film evaporation (TFE) technology. Wiper system ensures material residence time on Heated surface is short. The low-boiling component evaporates rapidly and passes through an entrainment separator. The entrainment separator knocks down liquid droplets; it minimizes liquid droplet carry-over. Vapors travel to an internal condenser and condense, uncondensed vapours then travel to an external condenser.

Placement of Internal Condenser ensures Vapour path is short & pressure drop is low. Such construction makes WFE into a Short Path Distillation Unit (SPDU) also known as Molecular Distillation Unit (MDU). In such construction vapours condense on the outside of the tubes and are discharged via the condensate outlet at the centre. , This makes the Short Path Distillation Unit (SPDU)/ Molecular Distillation Unit (MDU) technology the best choice for thermally sensitive materials. To name a few such chemicals as APIs, Cannabinoids, Dimer, Vitamin E / Tocopherol enrichment, and High-value oleoresins, Herbal / Natural extracts, etc.


The high-boiling residue flows along the shell wall under the action of gravity and wiper-assisted downward flow and is discharged from the Concentrate outlet. Different rotor designs are available to suit different feeds and their properties.


We can offer different configurations of Wiped Film Evaporators (WFEs) such as

a) Standard WFE with or without internal condenser

b) WFE with larger internal condenser

c) WFE with conical bottom and vapour outlet from top

d) WFE mounted on receivers

e) WFE with specially engineered rotor (different types of wiper systems - standard wipers, hinge type, swing type, metal blade, etc.)

Wiped Film Evaporator
Milestones
Manufactured 20 m2 WFE
Set up process to recover base oil from used lube oil & sold WFE of size 5 & 10 m²
Made a success of WFE for concentration of oleoresin to low PPM levels of solvents in the Concentrate
Exported 10 WFEs for Reclaiming Used Lube Oil
Manufactured WFE in 904L, Hastelloy, C276, C22.
Advantages of Wiped Film Evaporator (WFE)
  • Evaporation at very low operating temperatures — ideal for heat-sensitive products
  • Extremely short residence time (typically only a few seconds) again ideal for heat-sensitive products
  • High heat transfer coefficients (high-productivity equipment)
  • Low pressure drop on the vapour side — critical for efficient short path distillation
  • No degradation or loss of active ingredients
  • Self-cleaning of the heat transfer surface
  • Continuous single-pass & steady state operation (consistent performance)
  • Low maintenance
Wiped Film Evaporator
Features
  • Low rotational speed
  • No bottom bearing — simpler maintenance and reduced contamination risk
  • Louvers/chevron rotor with interchangeable panels for ease of cleaning
Falling Film Evaporator (FFE)

The Falling Film Evaporator (FFE) is the preferred choice for the continuous, efficient concentration equipment for dilute feed streams, usually before WFE applications. As established falling film evaporator manufacturer, Dalal Engineering designs FFE systems that use steam, hot water, or hot oil as the heating medium, operating under either atmospheric or vacuum conditions. Feed liquid enters at the top of the vertical tube bundle; the feed distributor ensures uniform wetting of every tube, and the liquid descends as a thin falling film. Due to indirect heat from outside and vacuum from inside, evaporation starts, and vapours and the liquid films both travel downwards. Resulting in heat transfer coefficients significantly superior to those of conventional shell-and-tube or reactor-based evaporators. Usually a recirculation mode of operation is used and sometimes a once-through.

The FFE is ideal as a pre-concentration stage before the feed is transferred to a WFE for final concentration. This staged approach reduces the thermal load on the downstream thin film evaporator, optimizing energy consumption and improving overall system economics. (Lower capex and lower opex)

Falling Film Evaporator
Total Solutions

Dalal Engineering supplies complete systems consisting of one or more Wiped Film Evaporators (WFE), Falling Film Evaporators (FFE), condensers, receivers for residue and concentrate, and vent condensers.

A pilot plant Wiped Film Evaporator (WFE) system is available at the Thane factory, where trials can be conducted to determine evaporation feasibility. Thereafter, WFE can be offered with process performance warranty.

WFE sizes & dimensions
Evaporator area m2 0.45 1.0 2.0 3.0 5.0 7.5 12.0 20.0
A (Square Cut-Out) 660 1010 1010 1320 1320 1320 1650 1895
B 1190 1710 1760 1800 1885 2249 2604 3360
C 616 1295 1770 1460 2205 2877 3590 5155
D 480 900 1200 1130 1190 2600 3000 2050
E 600 1000 1900 1690 2100 3000 3625 4000
Other sizes available as per requirement. Internal condenser optional.

Supertor — High-Shear Pump Mixer

Introduction

Supertor is a high shear pump like machine to handle Liquids & Slurries. It has saw tooth construction Stator & Rotor arrangement (close clearance stator and rotor). Rotary action creates high turbulence which is used for achieving - Homogenizing, Grinding, Crushing, Delumping, Dissolution, Maceration, etc.

Working Principle

The Supertor can crush, grind, homogenize & pump. An angular disc rotates in a cylindrical housing. Notched teeth in the Rotor disc meshes with teeth of Stator to effect disintegration & crushing - thus resulting movement generates thrust & shear causing acceleration of medium in both – axial & radial direction, resulting in intense mixing with pumping of the material.

Supertor Applications

Supertor is successfully is used in application such as high speed dispersers or batch emulsification / mixing, the Supertor operates continuously in Circulation or some times inline, reducing cycle times and enabling integration into automated process lines. It is equally effective as an inline homogenizer for emulsification of immiscible liquids and as an emulsification machine for producing stable emulsions at scale. The machine also supports wet micronization and particle micronization workflows, where surface-area enlargement through grain-size reduction is required to accelerate dissolution or reaction rates.

  • Mixing Fluids of various viscosities
  • Dispersing of pigments to produce colour
  • Rapid homogenisation and slurry formation from wet cake
  • Processing of pulp and black liquor in the paper Industry
  • Mixing & crushing of liquid and paste like waste materials
  • Surface enlargement through reduction in grain size for the dissolving process to reduce the dissolving time
  • Crushing of coke particles in thick tar in coking plant ancillaries
  • Increasing productivity and through put of spray dryers
  • Rapid reslurry of filter cakes for efficient washing , also increasing reaction rate
  • Waste cut treatment in the manufacture of fibre cement
  • Diverse extractions for manufacturing essences
  • Mixing & homogenising of spice extracts
  • Prevention of choking and clogging of pipelines
  • Clay & Silica application
  • Starch manufacture
  • Rapid dissolution of difficult-to-dissolve solids
  • Maceration

Dimensions
Size Suction Discharge L W H
22 100 100 1000 1020 497
25 150 150 1120 1250 572

Vibro Energy Seperators

Introduction

Vibro Energy Separators screen and grade dry powders and slurries with high efficiency across a broad range of industries - including abrasives, ceramics, chemicals, pharmaceuticals, powder coatings, minerals, metal powders, and food products. The machine's proven design delivers reliable, repeatable separation performance with minimal operator intervention.

Working Principle

The separator is a rigid screening device that vibrates about its center of mass. Eccentric weights mounted on both ends of a heavy-duty motor shaft generate controlled vibration. The amplitude and material flow pattern can be tuned by adding or removing auxiliary weights and by varying the angular offset between the top and bottom eccentric weights.

Salient Features
  • Low power, space and maintenance requirements
  • High separation efficiency
  • Separation achieved using meshes as fine as 500 mesh
  • Multi-deck arrangements with up to 7 decks for special applications

Technical Specifications
Size Motor
HP/KW
A
(mm)
B
(mm)
C
(mm)
D
(mm)
E
(mm)
F
(mm)
G
(mm)
H
(mm)
I
(mm)
J
(mm)
48 cms 0.25/0.186 495 450 695 580 810 1000 1130 100 554 360
66 cms 1/0.75 673 600 875 745 1005 1160 1245 127 740 482
80 cms 1/0.75 813 510 802 665 939 1100 1210 150 898 582
120 cms 2/1.5 952 520 872 705 1040 1233 1343 152 1195 730
150 cms 2/1.5 1105 535 885 710 1075 1265 1375 203 1502 927

Trial Facility

A pilot plant system is available at the Thane factory, where trials can be conducted to determine feasibility, and equipment with guaranteed performance can be offered.

After knowing application details and acceptance criteria, an evaporation feasibility study on the WFE pilot plant can be undertaken.

LAB SET UP

Wiped Film Evaporator (WFE)
Size M.O.C Qty. Required For Trial Qty. Of Samples Required For Testing Pressure Rating Remarks
0.45 m² SS-316 50 to 100 litres 200 Ltrs. Shell- Full vacuum Jacket – 6 kg/cm²g (steam) Typical throughput for aqueous material is about 60 to 100 kg/hr.
Parameters Vacuum – water Ring vacuum pump at approx. 700 mm Hg. Piston Pump with Booster – 0.5 mm Hg A.
Hot Media – Steam Heating – 100 to 180 ºC or Hot Oil Heating range 100 to 320 ºC
Cooling Media – Cooling Tower Water
ATFD
Size M.O.C Qty. Required For Trial Qty. Of Samples Required For Testing Pressure Rating Remarks
0.5m² SS-316 30 – 50 ltr/hr. 200 Ltrs. Shell- Full vacuum Jacket – 6 kg/cm²g (steam) Typical throughput for aqueous material is about 30 to 60 kg/hr.
Vibro Energy Seperators
Size M.O.C Qty. Required For Trial Qty. Of Samples Required For Testing Pressure Rating Remarks
19” dia SS-304 30 lit 20 to 50 kgs Meshes from 1/2” to 350 available. Throughput is in the region of 50 to 100 kg/hr depending upon particle size distribution.

Utilities Steam Boiler : 200 kg / hr, 6 kg / cm2g
Hot water Hot water circulation system is available with appropriate pump and temperature control.
Thermopack Suitable for, 320°C.
Vacuum a) 100 m²/hr. double stage water ring vacuum pump with air jet booster.
b) 100 m3/hr oil seal vacuum pump.
c) 125 m3/hr Rotary piston pump.
d) 1000 m3/hr Booster roots blower.
Cooling water a) Water at ambient temperature from cooling tower.
b) We can arrange chilled water circulation between 8 to 12° C for condensation of lower boiling materials.

LAB SET UP
Wiped Film Evaporator (WFE)

The WFE pilot plant is well equipped for a wide operating range – vacuum up to 0.5 Torr, jacket heating up to 300°C.

  • Pilot plant WFE set up with hot water / steam heating
  • Pilot plant WFE set up with hot oil heating
  • Vacuum station – water ring pump, rotary piston pump, and booster
  • Thermic fluid heating system
  • Steam boiler
  • Hot water system
  • Cooling Tower

The sample quantity required for conducting an evaporation feasibility study is approx. 200 liters.

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